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胺·西·氯氰乳油的气相色谱分析
冯俊涛1, 王兴林1, 张 兴1
西北农业大学 无公害农药研究服务中心
摘要:
采用气相色谱法在一根柱子上对三元复配制剂30%胺·西·氯氰乳油中的有效成份进行分析,方法简便、准确,可用于制剂生产中的质量控制。该方法的变异系数:甲胺磷为0.38%,氯氰菊酯为4.46%,西维因为0.95%。方法回收率:甲胺磷为99.64%,氯氰菊酯为97.12%,西维因为99.30%。
关键词:  胺·西·氯氰乳油,气相色谱,分析方法
DOI:
分类号:O657.7
基金项目:陕西省自然科学基金资助项目
Research on the Analytical Method for An Xi Luqing EC
Fen Juntao Wang Xinglin Zhang Xing,Fen Juntao Wang Xinglin Zhang Xing,Fen Juntao Wang Xinglin Zhang Xing
Abstract:
This paper reports an analytical method of An Xi Luqing EC,a tri-insecticide mixture, by means of GC using primicarb as aninternal standard on a packed column(crammed with 1.5% QF-1 1.5% OV-101)under suitable GC situations with the deviant coefficiences of Methamidophots 0. 38%, Carbary l0. 95% and Cypermethrin 4. 46%. THe average recovery of Methamidophos is 99. 64%,Carbaryl 99. 3% and Cypermethrin 97. 12%
Key words:  analytical method, GC, An Xi Luqing EC

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