| 摘要: |
| 为了解沙棘压榨汁内漂浮物中脂溶性有色物质的成分,以黄龙沙棘鲜果为试样,用提取色素法;经溶剂提取和薄层色谱分离,得到8种有色物质,其中有一种对光比较稳定的黄色油状液体,经IR及H—NMR鉴定,谱图与有机物物理常数和光谱谱图册中油精的数据一致。又用UV测试,200～400nm无吸收峰;400～500nm有两处最大吸收峰。测定结果与相应谱图表明,经提纯的这种黄色油状液体是油精。 |
| 关键词: 沙棘,色素,油精,红外光谱(IR),核磁共振谱(H—NMR),紫外吸收光谱(VU) |
| DOI： |
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| ISOLATION OF TRIOLEIN FROM FRUITS OF HIPPOPHAE RHAMNOIDES OF HUANGLONG AND IDENTIFICATION OF ITS STRUCTURE |
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Jiao Xinqun Wang Qinglian Gong Baosen,Jiao Xinqun Wang Qinglian Gong Baosen,Jiao Xinqun Wang Qinglian Gong Baosen
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| Abstract: |
| In order to understand the compositions of coloured fat soluble substances in the floating matters in the pressed inice of Hippophae Rhamnoides, the fresh fruit of Hippophae Rhamnoides from Huang-Long was used as the materials to be extracted with solution using the pigment method, and with acetone , petroleum and then separated with thinlayer chromatography from which eight coloured substances were obtained, of which one yellowish oily liquid stable to light was identified using IR and H-NMR. The results were in agreement with the data of triolein with "Atlas of Spectral data and physical constant for organic compounds II" . Again, the substance was determined using UV, in 200-400 nm there were no absorbance peak values, but in 400-500 nm there were two highest absorbance peaks.The results and the corresponding spectral atlas showed that this yellowish oily liquid through purification was triolein. |
| Key words: Hippophae Rhamnoides,pigment,triolein ( alycetin trioleate acid),Infrared spectroscopy ( IR ),Nuclear magnetic resonance spectroscopy ( H-NMR ),Ultra violet spectroscopy ( UV ) |
