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超临界二氧化碳萃取花椒挥发油研究
何 军1, 郭红祥1, 陈毓荃1
西北农业大学 无公害农药研究服务中心
摘要:
在样品粒度为60目时,采取静态、动态萃取相结合的操作方式,研究了萃取压力、温度及CO2体积对花椒挥发油萃取的影响。结果发现,萃取压力为34. 475MPa,温度为55℃,CO2体积为30mL时,萃取花椒挥发油效果较好, 3因素的主次关系为:温度>CO2体积>压力。
关键词:  超临界CO2萃取,花椒,挥发油
DOI:
分类号:S785.13
基金项目:国家“948”引进技术资助项目(971059)
The study on the extraction of Zanthorylum bungeanum maxim volatile oil by supercritical carbon dioxide fluid
Abstract:
In this paper, a systematic method was used to optimize the supercritical fluid extraction (SFE) of Zanthorylum bungeanum maxim volatile oil.Overall 3 variables (pressure, temperature, CO2 dynamistic extracting volume) were considered. SFE optimize conditions: temperature 55℃, pressure 34. 475 MPa,CO2 dynamistic extracting volume 30mL.The primary and secondary relation of the three variables is: temperature >CO2 volume>pressure.
Key words:  supercritical carbon dioxide fluid extraction,Zanthorylum bungeanum maxim,volatile oil