| 摘要: |
| 以丙酮和丙二酸为原料，经四步反应制出6-甲基-4-羟基-2-吡喃酮，再与取代苯胺的重氮盐通过偶合和重排反应合成出8个哒嗪酮类化合物，其中5个为新合成化合物。这8个化合物的结构均经过了元素分析，IR和1H-NMR的验证。 |
| 关键词: 哒嗪酮 偶合反应 结构表征 |
| DOI： |
| 分类号: |
| 基金项目:西北农林科技大学重点科研专项基金资助项目(KD00-18) |
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| Synthesis of 6-methyl-1-substituted phenyl-1,4-dihydro-4-oxo-pyridazine-3-carboxylic acids |
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| Abstract: |
| 5 new pyridazinone compounds,together with 3 known pyridazinone compounds were synthesized throng coupling and rearrangement reactions from substituted phenyl diazonium salts and 4-hydroxy-6-methyl-2-pyrone which were prepared from malonamic acid and acetone via 4 steps.The structures of 8 compounds were determined by elemental analysis,IR,and 1H-NMR. |
| Key words: pyridazinone coupling reaction structure characterization |
