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用电感耦合等离子体发射光谱法测定牛、羊奶中的多种元素
程浦海1, 鲁安太2, 宋才炽1
1.中国科学院西北水土保持研究所;2.西北农业大学
摘要:
本文报导了一个测定奶中多种元素的新方法。样品经450℃灰化后,用6当量盐酸容解残渣,然后用电感耦合等离子体光谱仪同时测定溶液中 Ca、Mg、Fe、Sr、Ba、Zn、Mn、Cu、和 Al 的含量。文中讨论了观察高度和正向功率对谱线强度的影响,并确定了仪器工作的最佳折衷条件。结果表明,该方法适用于奶中无机元素的分析。
关键词:  奶,无机元素,发射光谱分析
DOI:
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Determination of Multi-elements in Milk from Cows and Goats by means of Inductively Coupled Plasma--atomic Emission Spectroscopy
Cheng Puhai,Lu Antai Northwestern Institute of Soil and Water Conservation,Academia Sinica Northwestern Agricultural University,Cheng Puhai,Lu Antai Northwestern Institute of Soil and Water Conservation,Academia Sinica Northwestern Agricultural University,Cheng Puhai,Lu Antai Northwestern Institute of Soil and Water Conservation,Academia Sinica Northwestern Agricultural University
Abstract:
This paper reported a new method used in the determination of multi-elements in milk.After the sampies were ashed at 540℃,residues were solved with a equivalents of hydrochloric acid.And then,the contents of Ca/Mg/Fe/Sr/Ba/Zn/Mn/Cu/Al in the solusion were determined by means of the inductively coupled plasma-atomic emission spectroscopy (ICP-AES).Also,this paper discussed the effects of observed height and positive power upon the strength of spectrum lines,and determined the best trade-off working conditions of the instrument.Results indicated that this method was adaptable to the analysis of inorganic elements in milk.
Key words:  milk,inorganic elements,emission spectrographic analysis