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用电感耦合等离子体发射光谱法测定牛、羊奶中的多种元素
程浦海1, 鲁安太2, 宋才炽1
1.中国科学院西北水土保持研究所;2.西北农业大学
摘要:
本文报导了一个测定奶中多种元素的新方法。样品经450℃灰化后,用6当量盐酸容解残渣,然后用电感耦合等离子体光谱仪同时测定溶液中 Ca、Mg、Fe、Sr、Ba、Zn、Mn、Cu、和 Al 的含量。文中讨论了观察高度和正向功率对谱线强度的影响,并确定了仪器工作的最佳折衷条件。结果表明,该方法适用于奶中无机元素的分析。
关键词:  奶,无机元素,发射光谱分析
DOI:
分类号:
基金项目:
Determination of Multi-elements in Milk from Cows and Goats by means of Inductively Coupled Plasma--atomic Emission Spectroscopy
Cheng Puhai,Lu Antai Northwestern Institute of Soil and Water Conservation,Academia Sinica Northwestern Agricultural University
Abstract:
This paper reported a new method used in the determination of multi-elements in milk.After the sampies were ashed at 540℃,residues were solved with a equivalents of hydrochloric acid.And then,the contents of Ca/Mg/Fe/Sr/Ba/Zn/Mn/Cu/Al in the solusion were determined by means of the inductively coupled plasma-atomic emission spectroscopy (ICP-AES).Also,this paper discussed the effects of observed height and positive power upon the strength of spectrum lines,and determined the best trade-off working conditions of the instrument.Results indicated that this method was adaptable to the analysis of inorganic elements in milk.
Key words:  milk,inorganic elements,emission spectrographic analysis