| 摘要: |
| 以3,5-二羟基苯甲酸为原料,经Pd/C[w（Pd）=5%]催化转移加氢合成3,5-二氧代环己烷羧酸,然后酯化生成3-乙氧基-5-乙氧羰基-2-环己烯酮,最后水解得到3,5-二氧代环己烷羧酸乙酯.各产物通过1HNMR和GC-MS得以确认. |
| 关键词: 3，5-二氧代环己烷羧酸 3，5-二氧代环己烷羧酸乙酯 3-乙氧基-5-乙氧羰基-2-环己烯酮 有机合成 |
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| Synthesis method improvement of 3,5-Diketo-1-carbethoxycyclohexane |
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| Abstract: |
| 3,5-Dioxocyclohexanecarboxylic acid was prepared from 3,5-dihydroxybenzoicacid through transfer hydrogenation with 5% Pd/C as catalyst.3,5-diketo-1-carbethoxycyclohexane has been prepared through hydrolysis of 3-ethoxy-5-carboethoxy-2-cyclohexenon-e which was synthesized from 3,5-dioxocyelohexanecarboxylic.The structures were confirmed by 1HNMR and GC-MS. |
| Key words: 3,5-dioxocyclohexanecarboxylic 3,5-diketo-1-carbethoxycyclohexane 3-ethoxy-5-carboethoxy-2-cyclohexenone organic synthesis |
